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化學工業品-醇類分析方法應用

更新時間:2010-05-05點擊次數:5688

 

醇類
載氣:氦氣,30cm/sec,40 ℃時測定
柱箱溫度:40℃保持2min
          40—260℃,10℃/min
          260℃保持3min
進樣口:分流1:10,250℃
        0.01-0.05%的CS2溶液,進樣1μL
檢測器:FID,300℃
氮氣尾吹氣:30ml/min
氣相色譜柱:DB-624-Prosteel
            30m柱長×0.53mm內徑 3μm膜厚
譜圖:

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